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What is Penetration Grade Bitumen
Penetration grade Bitumen is a standardized classification system used to categorize bitumen based on its penetration value, which measures the depth (in tenths of a millimeter) to which a standard needle penetrates a sample of bitumen under specific conditions of time, temperature, and loading. The penetration value indicates the hardness or softness of the bitumen.
In the penetration grading system, common grades include Penetration Grade 60/70, 80/100, …… and 120/150. The first number represents the penetration value in tenths of a millimeter at 25°C, and the second number represents the penetration value at 25°C after the bitumen has been aged for a certain period of time, typically five hours.
Higher penetration values indicate softer bitumen, which is suitable for use in warmer climates, while lower penetration values indicate harder bitumen, which is suitable for use in colder climates. Penetration grade bitumen is commonly used in road construction for asphalt pavements, where the choice of grade depends on factors such as climate conditions, traffic loads, and pavement specifications.
What means of Bitumen 60/70?
Bitumen 60/70 refers to a specific grade of bitumen, which is a viscous, black, and sticky substance used in road construction and waterproofing. The numbers 60 and 70 represent the penetration value of the bitumen, indicating its hardness and viscosity. In this case, bitumen 60/70 means that the penetration value falls between 60 and 70, with lower values indicating harder bitumen and higher values indicating softer bitumen.
Penetration Grade Bitumen Production Process
The production process of penetration grade bitumen involves several stages, including refining crude oil, vacuum distillation, and quality control measures. Here’s a simplified overview of the production process:
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- Crude Oil Distillation: The process begins with crude oil being distilled in a refinery. Crude oil contains various hydrocarbon fractions, including bitumen. During distillation, crude oil is heated in a fractionating column, separating it into different components based on their boiling points. Bitumen, being one of the heavier fractions, is separated from lighter fractions such as gasoline and diesel.
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- Vacuum Distillation: Bitumen obtained from crude oil distillation is further processed through vacuum distillation to remove lighter hydrocarbons and impurities. Vacuum distillation is conducted under reduced pressure to lower the boiling points of the remaining components, preventing thermal cracking and degradation of bitumen.
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- Blending and Modification: Depending on the desired grade and application, bitumen may undergo blending with additives such as polymers, antioxidants, or solvents to modify its properties. Blending helps adjust the penetration value and other characteristics of the bitumen to meet specific requirements for road construction, waterproofing, or industrial use.
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- Quality Control and Testing: Throughout the production process, quality control measures are implemented to ensure that the bitumen meets specified standards and requirements. Testing is conducted to assess properties such as penetration, softening point, ductility, and performance characteristics. Quality control ensures consistency and reliability in the final product.
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- Packaging and Distribution: Once the bitumen is produced and tested, it is packaged into various containers such as drums, tanks, or bulk shipments for distribution to customers. Packaged bitumen is transported to construction sites, industrial facilities, or storage facilities for further use in road construction, roofing, waterproofing, and other applications.
Penetration Grade Bitumen Other Names
Penetration grade bitumen is also known by various other names depending on regional variations and industry terminology. Some common alternative names for penetration grade bitumen include:
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- Asphalt Cement
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- Bitumen Binder
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- Asphalt Bitumen
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- Road Bitumen
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- Petroleum Asphalt
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- Paving Grade Bitumen
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- Bituminous Binder
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- Road Tar
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- Asphaltic Bitumen
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- Construction Bitumen
These terms are often used interchangeably to refer to bitumen used in road construction, pavement surfacing, waterproofing, and other industrial applications.
Penetration Grading Benefits
The penetration grading system for bitumen offers several benefits:
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- Standardization: Penetration grading provides a standardized classification system for bitumen based on its penetration value, allowing for consistent characterization and specification of bitumen properties across different regions and industries. This standardization facilitates communication, quality control, and product performance evaluation.
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- Performance Prediction: The penetration value correlates with bitumen’s hardness or softness, which influences its performance characteristics such as resistance to deformation, rutting, cracking, and aging. Engineers and researchers can use penetration values to predict the behavior of bitumen under different loading and environmental conditions, helping optimize pavement designs and material selection.
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- Application Specificity: Different penetration grades of bitumen are tailored to suit specific climate conditions, traffic loads, and construction requirements. Engineers and contractors can select the appropriate grade of bitumen based on factors such as pavement design, temperature variations, and durability requirements, ensuring optimal performance and longevity in various applications.
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- Quality Assurance: By categorizing bitumen based on penetration values, the grading system helps ensure that bitumen products meet specific performance requirements and quality standards. Quality assurance measures can be implemented to verify that the bitumen complies with the specified penetration grade, ensuring reliable and consistent performance in construction and industrial applications.
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- Cost-effectiveness: Selecting the most suitable penetration grade of bitumen for a given application can lead to cost savings by optimizing material usage, reducing maintenance needs, and extending pavement service life. Matching bitumen properties with specific project requirements helps minimize over-engineering and unnecessary expenditures.
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- Compatibility: Penetration grading ensures compatibility between different batches of bitumen and asphalt mixes used in construction projects. Contractors can confidently mix and match bitumen from different sources, knowing that they conform to the same standardized grading system and performance specifications, thus promoting consistency and uniformity in construction practices.
Penetration Grading Components and Materials
The penetration grading of bitumen is primarily based on two components: penetration value and temperature susceptibility.
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- Penetration Value: This is the depth (in tenths of a millimeter) to which a standard needle penetrates the bitumen sample under specific conditions of time, temperature, and loading. The penetration value indicates the hardness or softness of the bitumen, with higher values indicating softer bitumen and lower values indicating harder bitumen.
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- Temperature Susceptibility: Penetration grading also takes into account the temperature susceptibility of bitumen, which refers to how the bitumen’s properties change with temperature variations. This is crucial because bitumen undergoes temperature fluctuations during its service life, and its performance must be predictable across different temperature ranges.
In addition to these components, the materials used in penetration grading include:
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- Bitumen Samples: Bitumen samples are obtained from refineries or asphalt plants and subjected to penetration testing to determine their penetration value and temperature susceptibility.
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- Standard Penetration Test Apparatus: This apparatus consists of a penetrometer and a standard needle used to measure the depth of penetration into the bitumen sample under controlled conditions of temperature and time.
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- Temperature Control Equipment: Temperature control equipment, such as ovens or temperature baths, is used to maintain the specified testing temperature during penetration testing.
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- Testing Standards and Specifications: Various testing standards and specifications, such as ASTM D5 and AASHTO M20, outline the procedures and requirements for penetration grading of bitumen, ensuring consistency and accuracy in testing procedures.
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- Data Analysis Tools: Data analysis tools and software may be used to interpret the results of penetration testing, calculate penetration values, and assess temperature susceptibility to determine the appropriate penetration grade of bitumen for specific applications.
Penetration Grade Bitumen Applications and Uses
Penetration grade bitumen finds extensive applications across various industries due to its versatility and performance characteristics. Some common applications and uses of penetration grade bitumen include:
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- Road Construction: Penetration grade bitumen is widely used as a binder in asphalt mixes for road construction, highway pavements, airport runways, and other transportation infrastructure projects. It provides durability, flexibility, and resistance to traffic loads, weathering, and environmental factors.
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- Pavement Surfacing: Bitumen is applied as a surface treatment or wearing course to improve the skid resistance, waterproofing, and longevity of road pavements. It forms a smooth, durable, and impermeable surface layer that protects the underlying pavement structure from moisture ingress, oxidation, and abrasion.
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- Roofing Materials: Penetration grade bitumen is used in the manufacturing of roofing materials such as built-up roofing membranes, roofing felts, and asphalt shingles. It provides waterproofing, weatherproofing, and thermal insulation properties, making it suitable for flat and sloped roof applications in residential, commercial, and industrial buildings.
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- Waterproofing: Bitumen is applied as a waterproofing membrane or coating in below-grade structures, basements, tunnels, bridges, and foundations to prevent water infiltration and protect against moisture-related damage. It forms a seamless, flexible, and durable barrier that seals cracks, joints, and penetrations, ensuring long-term structural integrity and moisture control.
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- Pavement Maintenance: Penetration grade bitumen is used for pavement maintenance and repair works, including pothole patching, crack sealing, and pavement rejuvenation. It provides adhesion, cohesion, and sealing properties that extend the service life of existing pavements and minimize the need for costly reconstruction.
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- Industrial Applications: Bitumen is utilized in various industrial applications such as pipe coating, corrosion protection, soundproofing, and vibration damping. It provides excellent adhesion, chemical resistance, and thermal stability in harsh operating conditions, making it suitable for use in pipelines, tanks, insulation materials, and automotive components.
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- Emulsions and Cutbacks: Bitumen emulsions and cutback bitumen are derived from penetration grade bitumen and used for specialized applications such as chip sealing, tack coating, fog sealing, and cold mix asphalt production. These modified bitumen products offer improved workability, adhesion, and curing properties, particularly in cold weather conditions.
Bitumen Penetration Grade Classification
Penetration grade bitumen is classified based on its penetration value, which indicates the hardness or softness of the bitumen. The classification typically follows the ASTM (American Society for Testing and Materials) or AASHTO (American Association of State Highway and Transportation Officials) standards.
Here is a common classification of penetration grade bitumen:
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- Penetration Grade 60/70: This grade of bitumen has a penetration value ranging from 60 to 70 tenths of a millimeter at 25°C. It is relatively soft and suitable for use in warm climates.
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- Penetration Grade 80/100: Bitumen in this grade has a penetration value ranging from 80 to 100 tenths of a millimeter at 25°C. It is slightly harder than 60/70 grade and is commonly used in moderate climates.
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- Penetration Grade 120/150: This grade of bitumen has a penetration value ranging from 120 to 150 tenths of a millimeter at 25°C. It is relatively hard and suitable for use in cold climates.
These are just examples of common penetration grade classifications. Depending on the region and specific standards, other penetration grade classifications may exist with varying penetration values and temperature susceptibilities. It’s important to consult the relevant standards and specifications to determine the appropriate penetration grade for specific applications and conditions.
The Major tests of penetration grade bitumen
The major tests conducted on penetration grade bitumen typically include:
1. Penetration Test: Measures the hardness of the bitumen by determining the depth in tenths of a millimeter to which a standard needle penetrates vertically in 5 seconds at a temperature of 25°C.
2. Softening Point Test: Determines the temperature at which the bitumen becomes soft enough to allow a steel ball to fall a specified distance under standard conditions.
3. Ductility Test: Evaluates the elongation properties of bitumen by measuring the distance a standard sample will stretch before breaking at a specified temperature.
4. Specific Gravity Test: Determines the density of bitumen compared to water, indicating its mass per unit volume.
5. Flash Point Test: Determines the lowest temperature at which vapors from the bitumen will ignite when exposed to a flame or spark.
These tests help ensure the quality and suitability of penetration grade bitumen for various applications, such as road construction and waterproofing.
Different Types of Penetration Bitumen Packaging
Penetration bitumen is commonly packaged in various forms to suit different transportation, storage, and application requirements. Some common types of penetration bitumen packaging include:
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- Drums: Penetration bitumen is often packaged in new steel drum with capacities ranging from 150 kg to 200 kg. Drums provide a convenient and portable packaging solution for smaller quantities of bitumen and are commonly used in road construction and maintenance projects.
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- Jumbo Bags: For larger quantities of bitumen, bulk bags or flexible intermediate bulk containers (FIBCs) are used. These bags have capacities ranging from 500 kg to 1500 kg and are typically made of woven polypropylene fabric. Bulk bags are suitable for bulk transportation and storage of bitumen and can be easily loaded onto trucks or containers.
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- Tanker Trucks: Liquid penetration bitumen is transported in tanker trucks or tank trailers equipped with insulated tanks. Tanker trucks have capacities ranging from 10,000 liters to 40,000 liters and are commonly used for bulk delivery of bitumen to construction sites, asphalt plants, and industrial facilities.
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- Bitutainer: Bitumen can also be transported in bitutainer, which are standardized shipping containers suitable for intermodal transportation via sea, rail, or road. Loading 25Ton per Bitutainer.
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- Flex tanks: Flex tanks are large, collapsible containers made of flexible polymer materials that can be used to transport and store liquid bitumen in bulk quantities. Flex tanks offer cost-effective and space-saving solutions for transporting bitumen over long distances and can be installed inside standard shipping containers for easy handling and loading.
- Bulk in Bitumen Carriers : We can supply Bulk Bitumen loading in Bulk Vessel (2000-30,000Ton)
Penetration grading key advantages and disadvantages are listed as below
Advantages | Disadvantages |
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The test is done at 25° C (77° F), which is reasonably close to a typical pavement average temperature. | The test is empirical and does not measure any fundamental engineering parameter such as viscosity. |
May also provide a better correlation with low-temperature asphalt binder properties than the viscosity test, which is performed at 60° C (140° F). | Shear rate is variable and high during the test. Since asphalt binders typically behave as a non-Newtonian fluid at 25° C (77° F), this will affect test results. |
Temperature susceptibility (the change in asphalt binder rheology with temperature) can be determined by conducting the test at temperatures other than 25° C (77° F). | Temperature susceptibility (the change in asphalt binder rheology with temperature) cannot be determined by a single test at 25° C (77° F). |
The test is quick and inexpensive. Therefore, it can easily be used in the field. | The test does not provide information with which to establish mixing and compaction temperatures. |
Penetration grades are listed as a range of penetration units (one penetration unit = 0.1 mm) such as 120 – 150. Penetration grades specified in AASHTO M 20 and ASTM D 946 are listed in below table
Penetration Grade | Comments |
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40 – 50 | Hardest grade. |
60 – 70 | Typical grades used in the U.S. |
85 – 100 | |
120 – 150 | |
200 – 300 | Softest grade. Used for cold climates such as northern Canada |
Penetration Grade Bitumen Specification (AASHTO M 20 and ASTM D 946)
Units | 40/50 | 60/70 | 80/100 | 100/120 | Test Methods | |
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Specific Gravity @25°C | – | 1.01-1.06 | 1.01-1.06 | 1.01-1.05 | 1.01-1.04 | ASTM D-70 |
Penetration @25°C, 100gm, 5sec | 0.1MM | 40-50 | 60-70 | 80-100 | 100-120 | ASTM D-5 |
Softening Point, Ring & Ball | °C | 52-60 | 49-56 | 45-52 | 42-49 | ASTM D-36 |
Ductility @25°C, after TFOT, Min | CM | 100 | 100 | 100 | 100 | ASTM D-113 |
Loss on Heating, Max | %Wt | 0.2 | 0.2 | 0.5 | 0.5 | ASTM D-6 |
Drop in Penetration after Heating, Max | % | 20.0 | 20.0 | 20.0 | 20.0 | ASTM D-6 & D-5 |
Flash Point Cleveland open cup, Min | °C | 250.0 | 250.0 | 232.0 | 250.0 | ASTM D-92 |
Solubility in CS2, Min | %Wt | 99.5 | 99.5 | 99.5 | 99.5 | ASTM D-4 |
Organic Matter Insoluble in CS2, Max | %Wt | 0.5 | 0.5 | 0.5 | 0.5 | ASTM D-4 |
Sport Test | – | Negative | Negative | Negative | Negative | A.A.S.H.O.T.102 |
Bitumen Specification European Standard (BS EN 12591)
Units | 35-50 | 40-60 | 50-70 | 70-100 | 100-150 | Test Methods | |
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Penetration @25°C, 100gm, 5sec | 0.1MM | 35-50 | 40-60 | 50-70 | 70-100 | 100-150 | EN 1426 |
Softening Point, Ring & Ball | °C | 50-58 | 48-56 | 46-54 | 43-51 | 39-47 | EN 1427 |
Resistace to Hardening@163°C | |||||||
– Change in mass, Max | %Wt | 0.5 | 0.5 | 0.5 | 0.8 | 0.8 | EN 12607-1 |
– Retained Penetration, Min | 0.1MM | 53 | 50 | 50 | 46 | 43 | |
– Softening point after hardinging, Min | °C | 52 | 49 | 48 | 45 | 41 | |
Other Properties | |||||||
Flash Point Cleveland open cup, Min | °C | 240 | 230 | 230 | 230 | 230 | EN ISO 2592 |
Solubility in CS2, Min | %Wt | 99.0 | 99.0 | 99.0 | 99.0 | 99.0 | EN 12592 |
Kinematic Viscocity @135°C, Min | mm2/S | 370 | 325 | 295 | 230 | 175 | EN 12595 |